If a crime is committed in the breaking of a window, these fragments may be used in evidence. Recent work in the characterisation of glass evidence by its elemental compo- sition, as opposed to traditional refractive index (RI) based methods, has required a framework for the. .
If a crime is committed in the breaking of a window, these fragments may be used in evidence. Recent work in the characterisation of glass evidence by its elemental compo- sition, as opposed to traditional refractive index (RI) based methods, has required a framework for the. .
Traditional methods of forensic glass analysis include the determination of a number of physical properties, including refractive index (RI), wet chemistry, scanning electron microscopy (SEM), x-ray fluorescence (XRF), and optical microscopy [1]. Although these techniques offer a high degree of. .
S. Montero, A. Hobbs, T. French and J.R. Almirall, “Elemental Profiling of Glass Fragments by ICP-MS as Evidence of Association: Analysis of a Case”, Journal of Forensic Sciences, 2003, 48(5) 1101-1107. Sources and thickness ranges of the known samples. S. Montero, A. Hobbs, T. French and J.R..
Elemental Analysis of Glass by SEM- EDS, XRF, LIBS and Laser Ablation-ICP- MS Elemental Analysis of Glass by SEM- EDS, XRF, LIBS and Laser Ablation-ICP- MS Jose R. Almirall Department of Chemistry and Biochemistry International Forensic Research Institute Florida International University Miami. .
Comparative analysis of glass fragments typically begins with microscopic examination. In this step, trace particles are selected for further comparative analysis. In most cases comparison material must also be prepared for the measurements. This is followed by determination of the refraction index. .
Previously the authors suggested the use of Hotelling's T2 statistic, a multivariate equivalent of Student's t-test, for determining a 'match' between glass fragments recovered from a suspect and a 'control' sample of glass fragments from the crime scene [I]. The use of Hotelling's T2 test was. .
Although the utility of trace elemental analyses and comparisons for glass and paint fragments by sophisticated methods such as laser ablation inductively coupled plasma (LA-ICP-MS) has been shown to offer a high degree of discrimination between different sources of these materials, the high.
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